Comments on: Diastereotopic Protons in 1H NMR Spectroscopy: Examples https://www.masterorganicchemistry.com/2022/02/08/diastereotopic-protons-1h-nmr-examples/ Tue, 05 Mar 2024 03:52:23 +0000 hourly 1 https://wordpress.org/?v=6.6.2 By: Najeeb Ullah https://www.masterorganicchemistry.com/2022/02/08/diastereotopic-protons-1h-nmr-examples/#comment-686584 Tue, 05 Mar 2024 03:52:23 +0000 https://www.masterorganicchemistry.com/?p=25602#comment-686584 I have faced problem i treated ethylenediamine with metal that form complex right. before complex ethylenediamine shows one triplet of CH2CH2 after complex formation its shows 2 duplets peak in different positions. So im confuse that before complexes formation the proton shows same behavior but after complex formation it shows different behavior. What is the reason please ?

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By: James Ashenhurst https://www.masterorganicchemistry.com/2022/02/08/diastereotopic-protons-1h-nmr-examples/#comment-643572 Fri, 02 Dec 2022 03:02:03 +0000 https://www.masterorganicchemistry.com/?p=25602#comment-643572 In reply to AH.

No, not as big as 1 ppm. That would be huge. It depends, but 0.1 to 0.2 ppm would be typical.

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By: AH https://www.masterorganicchemistry.com/2022/02/08/diastereotopic-protons-1h-nmr-examples/#comment-643531 Thu, 01 Dec 2022 14:33:57 +0000 https://www.masterorganicchemistry.com/?p=25602#comment-643531 Thanks for the article. How distinct would the chemical shifts be? Are we talking within 1PPM, or within 5PPM for example?
Thank you.

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